A new indirect AAS method using the bismuth phosphomolybdate complex for the
determination of phosphorus in foodstuffs is suggested. The bismuth
phosphomolybdate complex in acid medium was extacted with isobutyl
methylketone and the phosphorus was determined through bismuth in an
air/acetylene flame by utilising the 223.06 nm resonance line of bismuth. The
interference caused by antimony and titanium can be neglected in the presence
of excess of bismuth. The detection limit of the method is 0.008 mg/mL of
phosphorus.
Electron transport properties of single-crystal GaAs were determined using the photoacoustic method with the transmission detection configuration. The excess-carrier lifetime, the front and the rear recombination velocity, and the coefficients of the carrier diffusion and the thermal diffusivity were determined by comparing experimental results and theoretical photoacoustic signals.
Far-infrared reflection spectra were determined, for the first time, for single crystals of guanidinium aluminium sulphate hexahydrate (GASH) and its solid solution for 5 mol.% chromium isomorph (GCSH). The infrared active transversal and associated longitudinal phonon frequency and the dielectric permittivity functions for E//C and E perpendicular to C have been determined using both Kramers-Kronig analysis and a fitting procedure based on a four-parameter model. The indices of refraction were also measured using the immersion method with Cargille liquid and the results were compared with data obtained by numerical analysis of reflectivity measurements. The optical transmission of the samples were measured in the visible range and three wide energy bands were observed at about 2.6 eV, 3 eV and 4.9 eV for GASH doped with Cr, below the conduction energy zone.
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