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A method for the preparation of new 3 nitro 1,2,4 triazole derivatives has been suggested based on modification of the N hydroxymethyl group by nitration and nucleophilic substitution reactions. Thermal stability of 3 nitro 1,2,4 triazole N nitroxy and N azidomethyl deriva tives, as well as of dinitrates, 5,5´ dinitro 2,2´ bisnitroxymethyl 2H,2´H 3,3´ bi(1,2,4 triazole) and (nitromethylene)bis(1,2,4 triazole), has been studied.

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