For the application of chemical assessment standards by the extent of diagenetic alteration, we investigated three archaeological animal bones and a modern animal bone using Fourier transform infraredattenuated total reflection (FTIR-ATR) spectroscopy and x-ray diffraction (XRD) analysis. The calculating results of crystallinity index (CI), carbonate-to-phosphate (C/P) and carbonate-to-carbonate (C/C) using FTIR-ATR spectra showed differences CI and C/P according to the preservative condition of animal bones. By comparison of the crystallinity contents using XRD patterns, the states of animal bones were distinguished to the range of 30°-35°. As results of FTIR-ATR and XRD analysis, it is suggested that Mongolian large mammals bone presents the best preservative condition, and cattle bone from Naju site, and Haman site followed. In addition,
We studied for the chemical characterizations of the charred residues obtained from the ancient potteries in the Proto-Three Kingdom period from archaeological sites in Joong-do, Chuncheon. Organic components of the charred residues were extracted and analysed using mass spectrometry and infrared spectroscopy. Lipid profiles from these samples were not identified in gas chromatography-mass spectrometry. Bulk stable isotope analyses of charred residues was used to infer an average values of the foods prepared. The average carbon isotope values (δ 13 C) of the residues are -14.7±2.8‰ (ranging from -8.7‰ to -18.4‰, n=9), and nitrogen isotope values (δ 15 N) are 6.2±1.1‰ (ranging from -4.4‰ to -7.6‰, n=9). This is the first approach to analyse charred residues using stable isotopic method in Korea. Charred food residues on the interior surface of archaeological pottery can provide valuable information about pottery use and dietary habits of its population.
The analysis of ancient DNA extracted from archaeological bones has become an important research tool in palaeogenetics and anthropology. Eight human skeletal remains of the Joseon dynasty, excavated from Hwamyeong-dong, were used in this study. DNA was extracted from bone powder using a silica-based protocol. The isolated DNA was analyzed by the sequencing variation of hyper-variable region of the mitochondrial DNA. In the present study, 3 human remains were identified into mtDNA haplogroups including the A 5a, D4a, and M4"67+16311 groups, using HaploGrep 2 program. The identified haplotypes of the 3 samples have been confirmed that the specimens in the tombs were not related by the maternal line. This is the first analysis of human skeletal remains of the Joseon dynasty excavated in Busan. Date from the analysis of human remains from the Joseon dynasty are considered as the basis for understanding the genetic relationship between modern and ancient humans of the Korean peninsula.
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