In this study, graphite nanoplatelets (GNPs) were dispersed in a copolymer matrix consisting of bisphenol‐A based benzoxazine (BZ) and bi‐functional cycloaliphatic epoxy (CER), using two solvent‐free techniques: ultrasonication and three‐roll mill (3RM). The effects of GNP addition on the tensile performance, storage modulus, glass‐transition temperature (Tg), and electrical conductivity were evaluated. A maximum increase of nearly 46% and 20% in tensile modulus and strength, respectively, was found at 1.8 wt% of GNP content dispersed using the ultrasonication technique. In comparison, a superior enhancement with 55% and 37% increase in the tensile modulus and strength could be obtained at a lower GNP content, 0.9 wt%, dispersed via 3RM calendering, respectively. In the electrical conductivity measurement, a percolation threshold was achieved in the range between 0.6 wt% and 0.9 wt% of GNP content using the 3RM technique, which was in agreement with the predicted values. The theoretical stiffness obtained from the simplified Halpin‐Tsai model corresponded with the experimental data at low fractions. The incorporation of GNPs into the BZ/CER copolymer resulted in the full recovery of all the performance losses from the addition of CER to BZ. Choosing a proper dispersing technique, the 3RM calendering in this case, could lead to a minimum required GNP content for achieving superior nanocomposite performances.
A new plasma processing-based methodology for enhancing the streaming potential (V s ) that may be obtained in electrokinetic flows for a given pressure gradient over a silicon surface-based microchannel is indicated. The dependence of the V s on both the surface zeta potential and the electrolyte slip length was carefully determined through a series of experiments involving the variation of CF 4 -and Ar-based plasma parameters, incorporating pressure, exposure time, and power. It was determined through analytical estimates that, while the zeta potential is always increased, the slip length may be diminished under certain conditions. A record value of ∼0.1 mV/Pa was obtained using CF 4 plasma at 500 W, 10 mTorr, and 300 s of exposure. The implications of the work extend to the investigation of whether smooth surfaces may be effective for generating large V s 's for new modalities of electrical voltage sources in microfluidics-based applications.
The design, construction, and testing of a reentrant metal seal are described. The principal advantages of this seal are that it occupies a minimum cross-section diameter, requires no special alignment of the components, does not need a large rotational torque to seal, and has a large margin of sealing force. Jackscrews are used to apply the sealing force.
An eight-shot pneumatic pellet injection system has been developed for plasma fueling of the tokamak fusion test reactor (TFTR). The active cryogenic mechanisms consist of a solid hydrogen extruder and a rotating pellet wheel that are cooled by flowing liquid-helium refrigerant. The extruder provides solid hydrogen for stepwise loading of eight holes located circumferentially around the pellet wheel. This design allows for three different pellet diameters: 3.0 mm (three pellets), 3.5 mm (three pellets), and 4.0 mm (two pellets) in the present configuration. Each of the eight pellets can be shot independently. Deuterium pellets are accelerated in 1.0-m-long gun barrels with compressed hydrogen gas (at pressures from 70 to 105 bar) to velocities in the range 1.0–1.5 km/s. The pellets are transported to the plasma in an injection line that incorporates two stages of guide tubes with intermediate vacuum pumping stations. A remote, stand-alone control and data-acquisition system is used for injector and vacuum system operation. The eight-shot injection system has been installed and operated on TFTR. The design features, operation, and performance characteristics of the system are described.
scite is a Brooklyn-based organization that helps researchers better discover and understand research articles through Smart Citations–citations that display the context of the citation and describe whether the article provides supporting or contrasting evidence. scite is used by students and researchers from around the world and is funded in part by the National Science Foundation and the National Institute on Drug Abuse of the National Institutes of Health.