Highly dense AlN/CNT composite ceramics with 1-10% volume fractions of CNT were fabricated by spark plasma sintered (SPS) at 1400°C-1700°C. The results indicated that origination diameter of AlN had a great effect on microstructure and thermal conductivity. In details, for the system with AlN origination diameter of nanosized, the tubular structure of CNT has not been destructed, but when micro-sized AlN powder was adopted, the structure of CNT showed unstable at high temperature. Even though the degradation with incorporation of CNT into AlN, thermal conductivity of sintered AlN/CNT composites ceramics was evidently improved by adjusting content of additive Y2O3and the sintering process. Both the real part and imaginary part of the composites of Ka-Band (26.540.0 GHz) increase with the increase of CNT content, in which the increase of imaginary part is more than that of real part, resulting in an increase of loss factor. The AlN/ CNT thermal conductivity composites with appropriate CNT content and sintering temperature possess good dielectric dissipation and thermal conductivity.
AZ80 magnesium alloys were deformed at different temperature (270°C, 300°Cand 330°C)with different deformation ratio from 10% to 50%. The influence of varying the deformation temperature and ratio on the microstructure and hardness of AZ80 magnesium alloy was studied. The experimental results show that the hardness increased with the increasing of deformation and the hardness is up to the peak value with 40% deformation at 300°C. The microstructure was homogeneous and the grain was refined after hot deformation.The roles of both deformation strengthening and dispersition strengthening were to im prove the mechanical property of AZ80 magnesium alloy.
Finite element simulation of the effects of mould angle and friction condition on the equal channel angular pressing (ECAP) for AZ80 magnesium alloy were investigated by using DEFORM-3D program. The results show that the curve of load-displacement was divided into several stages including rapid increasing stage, load fluctuation, rapid increasing stage, steady stage and rapid drop stage. Firstly, when the angle decreased from 150°to 90°, the maximum load increased, and the same as energy consuming. In addition, the average effective strain increased with the decreasing of mould angle after single extrusion, while the degree of effective strain uniformity of the sample decreased and keep greater strain grads between inner and surface part. Secondly, the work load ascended with the increasing of the friction coefficient from 0 to 0.3, and one part of load overcome the friction and the other part is used for deformation of the sample. With the increment of friction coefficient, the average effective strain keeps steady value, while the degree of effective strain uniformity of the sample decreased. As mentioned above, large angle mould and low coefficient of friction should be adopted during ECAP deformation for AZ80 magnesium alloy.
continuous carbon fiber reinforced silicon carbide (Cf/SiC) ceramic matrix composites were prepared by precursor infiltration pyrolysis and chemical vapor infiltration (PIP-CVI process), in which the honeycomb sandwich structure preforms were fabricated by the three dimensional braid method. In this paper, the microstructure and the bending strength were observed and analyzed by SEM and three point bending method. The results of the study show that: The Cf/SiC ceramic matrix composites, which were lightweight and high strength, were prepared by that technique. The composite samples have a fiber volume fraction of 20%, a density of 0.38 g/cm3 and a flexural strength of 3.81 MPa. The honeycomb sandwich fiber reinforced ceramic matrix composite with a light weight, corrosion resistance and excellent physical and mechanical properties is a kind of structure and functional ceramic materials, which can realize the structure and the requirement of heat integration.
Fiber reinforced and aluminum phosphate-based composite was studied in this experiment. The composite was prepared through the process of lamination- hot press- sintering, binding material and fillers. The proper mixture ratio of Al2O3:AlPO4:H2O was 10:2.88:2.88.The slurry with this ratio was proper to prepare the composite. It indicated that the mechanical property of composite was excellent which was prepared by the slurry with this ratio. In order to improve the Mechanical property of silica glass fiber / aluminum phosphate composite, Al2O3 powders were graded in the slurry. Mechanical properties of composites were improved evidently.
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