Aiming at the problem that sapphire surface roughness is quite large after wet etching in sapphire microstructure processing technology, we optimize the wet etching process parameters, study on the influences of concentration and temperature of etching solution and etching time on the sapphire surface roughness and etching rate, choose different process parameters for the experiment and test and analyze the sapphire results after wet etching. Aiming at test results, we also optimize the process parameters and do experiment. Experimental results show that, after optimizing the parameters of etching solution, surface roughness of etched sapphire is 0.39 nm, effectively with reduced surface roughness, improved light extraction efficiency and meeting the production requirements of high-precision optical pressure sensor.
In this paper, we proposed an all-sapphire-based extrinsic Fabry-Perot interferometer (EFPI) pressure sensor based on an optimized wet etching process, aiming to improve the quality of the interference signal. The sapphire pressure sensitive diaphragm (SPSD) was fabricated by wet etching solutions with different mixture ratios of H3PO4 and H2SO4 at 280°C. The differences of mixture ratios affect the surface roughness of SPSD. SPSDs with surface roughness of 3.91nm and 0.39nm are obtained when the mixture ratios of H3PO4 and H2SO4 is 1:1 and 1:3, respectively. We constructed pressure sensing test system adopting these two kinds of SPSD and performed comparative test. The experiment results show that the demodulation jump can be solved and cavity length fluctuation is decreased to ±5nm when the surface roughness of SPSD is 0.39nm.
Aiming at the problem of heterogeneity of sealed cavity in silicon microstructure processing technology, the technology of preparing micro-cavity by using porous silicon sacrificial layer is proposed. The effect of current density on the preparation of porous silicon and the effect of porous silicon with different porosity on the formation of micro-cavity in the preparation process of porous silicon were studied. Different process parameters were selected for experiments and the prepared micro-cavities were tested and analyzed. According to the test results, the suitable electrochemical corrosion process parameters were selected to prepare porous silicon, and the micro-cavity was realized by changing the process parameters, which greatly increased the application fields of micro-sensors and micro-actuators.
Aiming at the problem of poor reliability of beam membrane fabrication in silicon microstructure processing technology, a technique for preparing microbeams using porous silicon sacrificial layer is proposed. The comparison of different porosity, different depths of porous silicon to beam membrane release and the comparison of different beam structures to beam membrane release were studied. The experiment was carried out by selecting different process parameters and testing the prepared beam membrane. According to the test results, the appropriate electrochemical corrosion process parameters were selected to prepare the porous silicon layer with appropriate porosity, large depth, good support effect and fast release speed, which can realize the release of the beam membrane and improve the reliability of the beam membrane. The field of application of microsensors and microactuators has been greatly increased.
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