Aim
The aim of the present study was to investigate the effectiveness of one total-etch self-priming adhesive and two one-step self-etching adhesive systems on the adhesion of a resin composite to both dentin and enamel. The effect of thermocycling on the adhesion was also investigated. The null hypothesis tested was thermocycling would not affect bond strengths to enamel and dentin treated with self-etching adhesives or a total-etch adhesive.
Methods and Materials
Two single-step self-etching adhesives [Xeno III (XE3) and Prompt L-Pop (PP)] and one two-step total-etch adhesive system (Prime & Bond NT) (P&B NT) were used in this study. Thirty cariesfree unrestored human third molars were used to make specimens of enamel and dentin. Different adhesives were applied on enamel and dentin surfaces according to the manufacturer's instructions then hybrid composite restorative material was condensed on the surface using a mold. The bonded specimens were stored in distilled water at 37°C for 24 hours before being tested. Half of the bonded specimens were tested for shear bond strength without thermocycling. The other half of the test specimens were thermocycled using a thermocycling apparatus in water baths held at 5°C and 55°C with a dwell time of one minute each for 10,000 cycles prior to shear testing. The mean shear bond strength before and after thermocycling was calculated, and the results were subjected to two-way analysis of variance (ANOVA) and repeated measure design to show the interaction between different materials and different times.
Results
The results showed shear bond strength on both enamel and dentin of the total-etch adhesive and the self-etching adhesives decreased after the specimens were subjected to thermocycling.
Conclusions
The null hypothesis tested “thermocycling would not affect bond strengths treated with selfetching adhesives” was rejected. Furthermore, the study revealed the following:
The shear bond strength to both enamel and dentin of the total-etch adhesive and the self-etching adhesives decreased after the specimens were subjected to thermocycling.
XE3 achieved the highest bond strength to both enamel and dentin (26.994±1.17 and 25.22±1.26, respectively).
XE3 showed even better bonding after thermocycling to enamel and dentin than the total-etching system or PP.
Although PP bonded to enamel showed lower shear bond strength value than XE3, it has durable bond strength even after thermocycling.
Citation
El Araby AM, Talic YF. The Effect of Thermocycling on the Adhesion of Self-etching Adhesives on Dental Enamel and Dentin. J Contemp Dent Pract 2007 February;(8)2:017-024.
There are many different ways to measure the bond strength of direct esthetic restorations to various dental substrates. Unfortunately, most methods cannot measure bond strengths immediately after a restoration has been placed. This lack of clinically-relevant information seriously affects the clinician's ability to select and use various bonding agents and procedures. The aim of this article is to provide a very detailed method for immediate measurement of in vitro bond strengths of direct bonded esthetic restorations. It focuses on the steps that o should be taken to select and prepare various tooth substrates for bond strength testing, the steps to "restore" various tooth substrates, and to measure the immediate in vitro bond strength. A fundamental understanding of o a standardized testing protocol should provide clinicians with a clearer appreciation of bond strengths associated with various bonding procedures.
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