Design and scale-up of a semi-industrial downer-reactor for the rounding of irregular polymer particles

Abstract

Abstract. The recent development of rapid prototyping technologies towards additive manufacturing reveals some major drawbacks of processes such as laser beam melting (LBM). This contribution focuses on the lack of suitable polymer material with a fine particle size and good flowability. Polymer particles obtained by a wet grinding process [1] are treated in a heated downer reactor. This treatment changes the particles' morphology from a chiselled state towards a spherical form by surface tension forces in a molten state [2] and leads to an improved flowability. To reach the required amount of rounded polymer powder, a downer reactor in semi-industrial scale has been established and will be characterized in this article. For the purpose of particle rounding it is necessary to avoid contact of molten particles with each other and with the hot reactor walls. Furthermore, the heat distribution has been investigated as one of the key parameters of the process. Finally, a proof of concept by rounding wet grinded PBT material was successfully conducted. The product was examined to obtain data about a change in particle size and flowability.

Spherical Polybutylene Terephthalate (PBT)—Polycarbonate (PC) Blend Particles by Mechanical Alloying and Thermal Rounding

“…The last cooling step is achieved at the lower unheated end of the reactor (1–0 m), where the obtained spherical particles are separated from the gas flow by means of a sintered metallic plate (SIKA-R20, GKN Sinter Metals GmbH, Radevormwald, Germany). A more detailed description of the geometry of the downer reactor has been reported previously [48].…”