Isolasi Metil Sinamat dari Minyak Atsiri Laja Gowah (Alpinia malaccensis (Burm.f.))

Riyanto, Arief; Yunilawati, Retno; Nuraeni, Chicha

doi:10.24817/jkk.v34i2.1859

Cited by 6 publications

(4 citation statements)

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“…Pada penelitian Amrullah et al (2017), dilakukan isolasi patchouli alcohol dari minyak nilam menggunakan alat spinning band distillation model 36-100 B/R Instrument, sedangkan Riyanto et al (2012) melakukan isolasi metil sinamat dari minyak atsiri laja gowah menggunakan alat spinning band distillation model 9400 B/R Instrument. Penelitian tersebut menjadi acuan pada tahapan penelitian ini, yaitu: karakterisasi minyak; analisis pergerakan suhu untuk menentukan suhu potong fraksi pertama, tekanan, laju panas, dan waktu kesetimbangan; serta penentuan rasio refluks dan suhu potong pada fraksi utama.…”

Section: Metodeunclassified

“…Pada penelitian ini, uji pergerakan suhu dilakukan untuk memvalidasi suhu penguapan aktual komponen-komponen minyak pada variabel yang digunakan (Riyanto et al, 2012). Laju panas akan memengaruhi kecepatan penguapan tiap komponen, semakin besar lajunya maka akan semakin cepat suhu naik.…”

Section: Hasil Dan Pembahasan Karakterisasi Minyakunclassified

“…Arum Nur Fitrah, Meika Syahbana Rusli, Dwi Setyaningsih, Arief Riyanto, Nur Hidayati Laju panas terpilih adalah 18 -16 -16% karena menghasilkan pergerakan suhu yang stabil (tidak cepat naik melewati 230 o C) sehingga diperoleh volume frakasi ringan yang cukup banyak. Jika laju pemanasan terlalu besar, suhu naik terlalu cepat sehingga komponen bertitik didih tinggi akan menguap bersama dengan komponen bertitik didih rendah, namun jika laju pemanasan terlalu kecil, proses akan berlangsung lama sehingga tidak efisien (Riyanto et al, 2012).…”

Section: Hasil Dan Pembahasan Karakterisasi Minyakunclassified

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Proses Pemurnian Fraksi Kaya Rhodinol Minyak Sereh Wangi Menggunakan Spinning Band Distillation

Fitrah¹,

Rusli²,

Setyaningsih³

et al. 2020

J.Tek.Ind.Pert.

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Indonesia, as one of the biggest countries which supplies citronella oil, has a high potential to produce natural rhodinol. Recent studies on rhodinol purification using fractional and mollecular distillation showed the difficulty of obtaining high purity and yield. The objective of this study was to determine the method of spinning band distillation to purify rhodinol regarding reflux ratio and vaporization temperature. Citronella oil was divided into three fractions according to its boiling points. The volume of each fraction was estimated by its ratio (according to GC analysis) to the feed volume: F1 (components before rhodinol) 21.73%, F2 (rhodinol) 61.7%, and residue 15.82%. Initial research established the best conditioning before the purification process was 3 mmHg of pressure, equilibration started at 160oC in 30 minutes, and 18–17% of heat rate, as these created the stability of the vapor temperature. The levels of reflux ratio were 3:1 and 5:1, while the evaporation temperatures of rhodinol were 230oC and 235 oC. Reflux ratio of 5:1 at 230oC obtained the highest purity (81.30%) and the highest yield (72.94%). Equilibration and reflux ratio allowed rectification inside the column because the spinning band homogenized the vapour molecules by its downwards flow and wiped the reflux on the inner surface, which in turn caused the molecules with a lower boiling point to evaporate gradually. Meanwhile the other yields were 79.81% (3:1 at 230 oC), 80.53% (3:1 at 235 oC), and 80.21% (5:1 at 23oC) with yields of 71.82%, 70.31%, and 68.23%. Keywords: citronella oil, purification, rhodinol, spinning band distillation

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Section: Metodeunclassified

Section: Hasil Dan Pembahasan Karakterisasi Minyakunclassified

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Proses Pemurnian Fraksi Kaya Rhodinol Minyak Sereh Wangi Menggunakan Spinning Band Distillation

Fitrah¹,

Rusli²,

Setyaningsih³

et al. 2020

J.Tek.Ind.Pert.

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“…Laja gowah oil is one of Indonesia's newly developed essential oil commodities with promising business prospects. The main content of laja gowah essential oil is methyl cinnamate, cineol, and α-pinene (Riyanto et al, 2012). Laja gowah oil is reported to have antibacterial activity against Gram-negative and Gram-positive bacteria (Sitorus & Satria, 2016).…”

Section: Introductionmentioning

confidence: 99%

Antibacterial activity of Laja Gowah (Alpinia malaccensis (Brum.f) Roscoe) oil in Reducing the Number of Staphylococcus aureus Colonies in Hospital Wards

Nisyak

2021

Trad.Med.J

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Staphylococcus aureus is one of the pathogenic bacteria that cause nosocomial infections in hospitals. The use of essential oil-based antibacterials for hospital wards was developed to prevent nosocomial infections. Laja gowah oil is an essential oil isolated from the Alpinia malaccensis plant, which belongs to the Zingiberaceae plant group. The purpose of this study was to determine the antibacterial activity of laja gowah oil in reducing the number of S. aureus colonies in hospital inpatient rooms through the air diffusion method. The compound content in laja gowah oil was analyzed with GC-MS. The study of antibacterial activity using the total plant counts continued with the colony count test, Gram staining, catalase test, and coagulase test. Laja gowah oil contains methyl cinnamate and 1,8-cineole. The installation time of the diffuser containing laja gowah oil affects the number of colonies of S. aureus bacteria in hospital wards. The antibacterial activity of laja gowah oil was influenced by the synergistic effect of methyl cinnamate and 1,8-cineole compounds.

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Biotransformation of compounds in laja gowah oil by Aspergillus niger and its antibacterial activity

Nisyak

Hisbiyah

Wardani

2023

The 8th International Conference and Workshop on Basic and Applied Science (Icowobas) 2021

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Isolasi Metil Sinamat dari Minyak Atsiri Laja Gowah (Alpinia malaccensis (Burm.f.))

Cited by 6 publications

References 0 publications

Proses Pemurnian Fraksi Kaya Rhodinol Minyak Sereh Wangi Menggunakan Spinning Band Distillation

Proses Pemurnian Fraksi Kaya Rhodinol Minyak Sereh Wangi Menggunakan Spinning Band Distillation

Antibacterial activity of Laja Gowah (Alpinia malaccensis (Brum.f) Roscoe) oil in Reducing the Number of Staphylococcus aureus Colonies in Hospital Wards

Biotransformation of compounds in laja gowah oil by Aspergillus niger and its antibacterial activity

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