2019
DOI: 10.3390/polym11030422
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The Structure and Properties of Polyacrylonitrile Nascent Composite Fibers with Grafted Multi Walled Carbon Nanotubes Prepared by Wet Spinning Method

Abstract: Polyacrylonitrile (PAN) grafted amino-functionalized multi walled carbon nanotubes (amino-MWCNTs) were synthesized by in situ polymerization under aqueous solvent. The grafted MWCNT/PAN nascent composite fibers were prepared by the wet spinning method. Fourier transform infrared spectroscopy and Raman spectroscopy indicated that the amino-MWCNTs and PAN macromolecular chains had interfacial interactions and formed chemical bonds. The grafting content of the PAN polymer on the amino-MWCNTs was up to 73.2% by th… Show more

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Cited by 23 publications
(12 citation statements)
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“…The Raman spectrum obtained from the PAN nanofiber mat exhibited two peaks at 1454 and 1077 cm −1 that were assigned to the bending vibrations of C−H groups. 36,37 The Raman spectrum of the Cu microfiber mat was consistent with that of the previously reported bare Cu, which has a broad peak between 1500 and 2500 cm −1 . 38 The peaks appearing between 0 and 750 cm −1 associated with the oxidation of Cu are not shown.…”
Section: Resultssupporting
confidence: 87%
“…The Raman spectrum obtained from the PAN nanofiber mat exhibited two peaks at 1454 and 1077 cm −1 that were assigned to the bending vibrations of C−H groups. 36,37 The Raman spectrum of the Cu microfiber mat was consistent with that of the previously reported bare Cu, which has a broad peak between 1500 and 2500 cm −1 . 38 The peaks appearing between 0 and 750 cm −1 associated with the oxidation of Cu are not shown.…”
Section: Resultssupporting
confidence: 87%
“…Among various polymer fiber fabrication techniques, wet spinning and electrospinning have been the most frequently applied methods in the recent years [6][7][8][9][10][11][12][13][14][15][16][17][18][19][20][21][22]. Known as a primary method, wet spinning has been employed to prepare a significant majority of PAN fibers [23][24][25][26].…”
Section: Introductionmentioning
confidence: 99%
“…Accordingly, research on conductive yarn based on spinning processes such as dry-jet spinning and wet spinning is steadily progressing by manufacturing a conductive nanofiller/polymer composite solution incorporating carbon nanofiller and metal nanowires in the polymer [3,6,7]. In particular, research on wet spinning for a carbon nanomaterial/polymer composite solution is in progress [8][9][10][11][12][13][14][15]. It is common to spinning a PAN polymer through wet spinning and does not require heat during the process.…”
Section: Introductionmentioning
confidence: 99%
“…Polyacrylonitrile (PAN) is one of the most important polymers for preparing high-performance carbon fibers. Recently, carbon nanomaterial/PAN composite fibers with improved mechanical properties from the carbon fibers have been produced [8][9][10][11][12][13][14][15].…”
Section: Introductionmentioning
confidence: 99%