Zur Kenntnis des Schellacks, IX. Mitteil.: Über die Konstitution der Aleuritinsäure

Nagel, W.; Mertens, Willi

doi:10.1002/cber.19360690910

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Separation Of Ustilic Acid Derivatives By Distillatio7z1

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1937

1969

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Cited by 8 publications

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“…of dry acetone and eight drops of conceiltrated sulphuric acid (26). The ustilic acids, which are only sparingly soluble in acetone, soon dissolved.…”

Section: Separation Of Ustilic Acid Derivatives By Distillatio7zmentioning

confidence: 99%

Biochemistry of the Ustilaginales: Viii. The Structures and Configurations of the Ustilic Acids

Lemieux¹

1953

Can. J. Chem.

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Methanolysis of ustilagic acid a r~d hydrolysis of the methyl esters for~lled yielded a crystalline acidic fraction which was essentially a mixture of two substances termed the ustilic acids A and B. The acids were separated as their isopropylidene derivatives. The ustilic acids cocrystallize to mixtures with melting points intermediate between those of the pure compounds. Conversion of ustilic acid A, 1n.p. 112-113" C., [O]D -8" in methanol, which made up about 70% of the mixture, by hydrogenolysis to palmitic acid, by oxidation with chromic oxide to pentadecanedioic acid, and by lead tetraacetate oxidation followed by hydrogenation to 15-hydroxypentadecanoic acid showed the substance to be a n optically active form of 15,16-dihyd

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“…of dry acetone and eight drops of conceiltrated sulphuric acid (26). The ustilic acids, which are only sparingly soluble in acetone, soon dissolved.…”

Section: Separation Of Ustilic Acid Derivatives By Distillatio7zmentioning

confidence: 99%

Biochemistry of the Ustilaginales: Viii. The Structures and Configurations of the Ustilic Acids

Lemieux¹

1953

Can. J. Chem.

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Zur Kenntnis des Schellacks, XIII. Mitteil.: Die Überführung der Aleuritinsäure in Hexadecensäure

Nagel

Mertens

1941

Ber. dtsch. Chem. Ges. A/B

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Untersuchungen über den Kork, IX. Die Konstitution der Phloion‐ und Phloionolsäure

Zetzsche¹

1938

J. Prakt. Chem.

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Zur Kenntnis des Schellacks, IX. Mitteil.: Über die Konstitution der Aleuritinsäure

Abstract: 4.988 mg Sbst. : 11.480 mg CO,, 4.450 mg H,O. -124.0 mg Sbst. : 164.4 mg AgJ.

Cited by 8 publications

References 3 publications

Biochemistry of the Ustilaginales: Viii. The Structures and Configurations of the Ustilic Acids

Biochemistry of the Ustilaginales: Viii. The Structures and Configurations of the Ustilic Acids

Zur Kenntnis des Schellacks, XIII. Mitteil.: Die Überführung der Aleuritinsäure in Hexadecensäure

Untersuchungen über den Kork, IX. Die Konstitution der Phloion‐ und Phloionolsäure

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