Stir casting is an economical process for the fabrication of aluminum matrix composites. There are many parameters in this process, which affect the final microstructure and mechanical properties of the composites. In this study, micron-sized SiC particles were used as reinforcement to fabricate Al-3 wt% SiC composites at two casting temperatures (680 and 850 °C) and stirring periods (2 and 6 min). Factors of reaction at matrix/ ceramic interface, porosity, ceramic incorporation, and agglomeration of the particles were evaluated by scanning electron microscope (SEM) and high-resolution transition electron microscope (HRTEM) studies. From microstructural characterizations, it is concluded that the shorter stirring period is required for ceramic incorporation to achieve metal/ceramic bonding at the interface. The higher stirring temperature (850 °C) also leads to improved ceramic incorporation. In some cases, shrinkage porosity and intensive formation of Al4C3 at the metal/ceramic interface are also observed. Finally, the mechanical properties of the composites were evaluated, and their relation with the corresponding microstructure and processing parameters of the composites was discussed.
AbstractStir casting is an economical process for fabricating aluminium matrix composites. There are
Due to a high propensity of nano-particles to agglomerate, making aluminium matrix composites with a uniform dispersion of the nano-particles using liquid routes is an exceptionally difficult task. In this study, an innovative approach was utilised to prevent agglomeration of nano-particle by encapsulating SiC nanoparticles using graphene sheets during ball milling. Subsequently, the milled mixture was incorporated into A356 molten alloy using non-contact ultrasonic vibration method. Two different shapes for graphene sheets were characterised using HRTEM, including onion-like shells encapsulating SiC particles and disk-shaped graphene nanosheets. This resulted in 45% and 84% improvement in yield strength and tensile ductility, respectively. The former was ascribed to the Orowan strengthening mechanism, while the latter is due primarily to the fiber pull-out mechanism, brought about by the alteration of the solidification mechanism from particle pushing to particle engulfment during solidification as a consequence of high thermal conductive graphene sheets encapsulating SiC particles. Due to a high propensity of nano-particles to agglomerate, making aluminium matrix composites with 13 a uniform dispersion of the nano-particles using liquid routes is an exceptionally difficult task. In this 14 study, an innovative approach was utilised to prevent agglomeration of nano-particles by
15encapsulating SiC nano-particles using graphene sheets during ball milling. Subsequently, the milled 16 mixture was incorporated into A356 molten alloy using non-contact ultrasonic vibration method. Two 17 different shapes for graphene sheets were characterised using HRTEM, including onion-like shells
18encapsulating SiC particles and disk-shaped graphene nanosheets. This resulted in 45% and 84%
19improvement in yield strength and tensile ductility, respectively. The former was ascribed to the
20Orowan strengthening mechanism, while the latter is due primarily to the fiber pull-out mechanism, 21 brought about by the alteration of the solidification mechanism from particle pushing to particle
ab s t r a c tIn this study, the hot extrusion process was applied to stir cast aluminum matrix-SiC composites in order to im-prove their microstructure and reduce cast part defects. SiC particles were ball milled with Cr, Cu, and Ti as three forms of carrier agents to improve SiC incorporation. Large brittle ceramic particles (average particle size: 80 μm) were fragmented during ball-milling to form nanoparticles in order to reduce the cost of composite manufactur-ing. The experimental results indicate that full conversion of coarse micron sized to nanoparticles, even after 36 h of ball milling, was not possible. Multi modal SiC particle size distributions which included SiC nanoparticles were produced after the milling process, leading to the incorporation of a size range of SiC particle sizes from about 50 nm to larger than 10 μm, into the molten A356 aluminum alloy. The particle size of the milled powders and the amount of released heat from the reaction between the carrier agent and molten aluminum are inferred as two crucial factors that affect the resultant part tensile properties and microhardness.
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