We present the design, realization, and performance of a three-axis vector nano superconducting quantum interference device (nanoSQUID). It consists of three mutually orthogonal SQUID nanoloops that allow distinguishing the three components of the vector magnetic moment of individual nanoparticles placed at a specific position. The device is based on Nb/HfTi/Nb Josephson junctions and exhibits line widths of ∼250 nm and inner loop areas of 600 × 90 and 500 × 500 nm(2). Operation at temperature T = 4.2 K under external magnetic fields perpendicular to the substrate plane up to ∼50 mT is demonstrated. The experimental flux noise below [Formula: see text] in the white noise limit and the reduced dimensions lead to a total calculated spin sensitivity of [Formula: see text] and [Formula: see text] for the in-plane and out-of-plane components of the vector magnetic moment, respectively. The potential of the device for studying three-dimensional properties of individual nanomagnets is discussed.
We analyze electric transport and noise properties at 4.2 K of self-shunted superconductor-normal metal-superconductor (SNS) sandwich-type Josephson junctions, comprising Nb as the superconductor and Hf-Ti as the normal conducting material, with lateral dimensions down to approximately 80 nm. The junctions are fabricated with an optimized multilayer Nb technology based on nanopatterning by electron-beam lithography and chemical-mechanical polishing. The dependence of transport properties on the junction geometry (lateral size and barrier thickness d Hf-Ti) is studied, yielding a characteristic voltage V c up to approximately 100 μV for the smallest d Hf-Ti = 17 nm. The observed small hysteresis in the current-voltage curves of devices with high V c and large size can be attributed to self-heating of the junctions and fitted with an extended version of the resistively shunted junction model. Measurements of voltage noise of single junctions are consistent with the model including self-heating effects. The potential of our technology for further miniaturization of nanoscale superconducting quantum interference devices and for the improvement of their performance is discussed.
In the recent past, considerable effort was spent on the development of superconducting quantum interference device (SQUID) designs for magnetic detection in the micro- and nano-scale. Where these novel nanoSQUIDs were mostly of a simple format, real applications require more elaborate designs including auxiliary components such as coils and transformers. Therefore, we have developed SQUID designs based on a Nb/HfTi/Nb thin-film technology which offers both, nano-patterning and waferscale manufacturing of complex design structures. Employing e-beam lithography and chemical–mechanical polishing process steps, the area of the superconductor–normal conductor–superconductor Josephson junctions of these nanoSQUIDs has been varied between 150 nm × 150 nm and 200 nm × 200 nm, whereas the thickness of the barrier is about 20 nm. In order to enable real practical applications, nanoSQUID designs with a number of implemented auxiliary components and design features, such as gradiometric feedback loops, gradiometric transformers, and rf filters, have been carefully investigated. This paper combines a summary of recent achievements with a presentation of detailed measurements of the device performance in magnetic fields of up to a few tens of millitesla. This investigation is intended to pave the way for future practical complex nanoSQUID tools.
Radon gas is the largest source of public exposure to naturally occurring radioactivity. However, radon is also a useful tracer for understanding atmospheric processes, assessing the accuracy of chemical transport models, and enabling integrated emissions estimates of greenhouse gases. A sound metrological system for low level atmospheric radon observations is therefore needed for the benefit of the atmospheric, climate and radiation protection research communities. To this end, here we present a new calibration method for activity concentrations below 20 Bq m−3 and a prototype of the first portable radon monitor capable of achieving uncertainties of 5% (at k = 2) at these concentrations. Compliance checking of policy-driven regulations regarding greenhouse gas (GHG) emissions is an essential component of climate change mitigation efforts. Independent, reliable ‘top down’ methods that can be applied consistently for estimating local- to regional-scale GHG emissions (such as the radon tracer method (RTM)) are an essential part of this process. The RTM relies upon observed radon and GHG concentrations and measured or modeled radon fluxes. Reliable radon flux maps could also significantly aid EU member states comply with European COUNCIL DIRECTIVE 2013/59/EURATOM. This article also introduces the traceRadon project, key aims of which include outlining a standardized approach for application of the RTM, creating infrastructure with a traceability chain for radon concentration and radon flux measurements, and developing tools for the validation of radon flux models. Since radon progeny dominate the terrestrial gamma dose rate, the planned traceRadon activities are also expected to improve the sensitivity of radiation protection early warning networks because of the correlation known to exist between radon flux and ambient equivalent dose rates.
We have fabricated Nb-based dc-SQUIDs with sub-micrometer planar Nb/HfTi/Nb junctions in order to investigate their noise performance. The SQUIDs are of simple coplanar design, their nominal inductance is ca. 15 pH. Electron beam lithography and chemical-mechanical polishing have been used to realize junctions with cross sections areas as low as about 100 × 100 nm2. The SQUIDs exhibit pronounced excess noise increasing towards lower frequencies. This apparent flux noise arises from fluctuations of the junction critical currents or resistances. The Nb/HfTi/Nb junction critical currents are found to be strongly temperature dependent. Upon cooling below ca. 4 K the SQUIDs start to show current–voltage characteristics with negative differential resistances, and their flux noise increases significantly. Estimation of the HfTi barrier electron temperature indicates that the degradation of the SQUID properties towards lower temperature is caused by self-heating effects.
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