A Green Analytical Method for the Multielemental Determination of Halogens and Sulfur in Pet Food

Mello, Julia Eisenhardt de; Novo, Diogo La Rosa; Coelho, Gilberto Silva; Scaglioni, Priscila Tessmer; Mesko, Márcia F.

doi:10.1007/s12161-019-01549-w

Cited by 15 publications

(10 citation statements)

References 20 publications

Supporting

Mentioning

Contrasting

Order By: Relevance

“…In this respect, IC-MS was adopted relatively rapidly in food science research and applications and related industries. Applications which saw the early adoption of IC-MS included detection of pesticide levels in commercial fruits, vegetables, and beverages; 48 − 54 sugar concentrations in dried bean crops; 55 herbicides in baby food commodities; 56 1-hydroxyethylidene-1,1-diphosphonic acid in uncooked food; 57 halogens and sulfur in pet foods; 58 and fosetyl and phosphonic acid in plant-derived matrices. 59 These studies demonstrate broad applications in food science largely driven by the competitive analytical performance, and sample preparation simplicity required by, IC-MS, combined with the polar and ionic nature of the analytes ( Table 1 ).…”

Section: Ic-ms Applicationsmentioning

confidence: 99%

Ion-Exchange Chromatography Coupled to Mass Spectrometry in Life Science, Environmental, and Medical Research

et al. 2023

View full text Add to dashboard Cite

Section: Ic-ms Applicationsmentioning

confidence: 99%

Ion-Exchange Chromatography Coupled to Mass Spectrometry in Life Science, Environmental, and Medical Research

et al. 2023

View full text Add to dashboard Cite

“…Then it was dried in an oven at 100-150 C for 6 hours and cooled again in a desiccator for 30 minutes. 16…”

Section: Water Contentmentioning

confidence: 99%

Phytochemicals, proximate composition, minerals and volatile oil analysis of Zanthoxylum acanthopodium DC. fruits

Satria

Dalimunthe²,

Pertiwi³

et al. 2023

F1000Res

View full text Add to dashboard Cite

Background: The use of herbal plants is adopted as a traditional medicine because of their minimal side effects. Most plants have bioactive ingredients and nutritional content that can potentially be used as treatments. One plant that has the potential to be a source of modern medicine is Zanthoxylum acanthopodium DC. Historically the use of traditional medicine as a treatment has enjoyed a good sense of trust among the public. The purpose of this study was to perform a qualitative phytochemical screening and proximate analysis of samples of Zanthoxylum acanthopodium DC. Methods: Used in this study were the phytochemical screening test using the thin-layer chromatography method and the proximate analysis using the AOAC method, which included measuring the ash, water, carbohydrate, total fat, protein, and crude fiber content of the samples. Hydrodistillation was used to isolate volatile oil from the sample, which was then identified using gas chromatography-mass spectrometry. The research method used is experimental. Results: From the test, it was found that the phytochemical content of Zanthoxylum acanthopodium DC is alkaloids, flavonoids, tannins, saponins, glycosides, steroids, and triterpenoids. Proximate analysis obtained ash content of 6.19%, water content of 6.35%, carbohydrates of 35.4%, total fat of 2.46%, protein of 16.2%, and crude fiber of 33.4%. Mineral test results prove that Zanthoxylum acanthopodium DC contains Pb (<0.07 mg/Kg), Cd (<0.03 mg/Kg), As (<0.03 mg/Kg), Hg (0.0011 mg/Kg), Mn (43.1 mg/Kg), K (321 mg/Kg), Ca (0.22 mg/Kg), Mg (198 mg/Kg), Fe (52.1 mg/Kg), and Na (23.6 mg/Kg). The highest content of essential oil in Zanthoxylum acanthopodium DC is geranyl acetate, with a concentration of 24.26%. Conclusions: This study concludes that the research findings of Zanthoxylum acanthopodium DC indicate that the phytochemical, mineral, and volatile oil content of the sample is strongly related to its potential to be developed as food and medicine.

show abstract

“…The new analytical flow path reduces the number of steps necessary, permits multicomponent analysis, and reduces the amount of chemicals. Simultaneously, the limits of detection and the sample throuput are improved compared to the AOAC International recommended methods 28,29 …”

Section: Food and Beveragesmentioning

confidence: 99%

Combining ion chromatography with mass spectrometry and inductively coupled plasma‐mass spectrometry: Annual review 2020

Bruggink¹,

Jensen

2020

Analytical Science Advances

View full text Add to dashboard Cite

The demand for analyzing low molecular weight polar and ionic components in body fluids, pharmaceutical formulations, food, environmental samples, and drinking water is increasing. Ion chromatography (IC) offers significant advantages over RPLC and HILIC due to a complementary chromatographic selectivity, a different retention mechanism, and a high tolerance toward complex matrices. A continuously regenerated membrane desalter simplifies the combination of IC‐applications with MS‐ or MS/MS‐detection, improving the sensitivity and specificity. Analytical workflows are streamlined, providing higher sample throughput. Combining IC with ICP‐MS simplifies the speciation analysis of inorganic and organic polar components. The knowledge about the distribution of an element among chemical species in a sample is essential due to significantly different toxicological or environmental properties. This annual review evaluates the literature published from late 2019 until November 2020.

show abstract

A Green Analytical Method for the Multielemental Determination of Halogens and Sulfur in Pet Food

Cited by 15 publications

References 20 publications

Ion-Exchange Chromatography Coupled to Mass Spectrometry in Life Science, Environmental, and Medical Research

Ion-Exchange Chromatography Coupled to Mass Spectrometry in Life Science, Environmental, and Medical Research

Phytochemicals, proximate composition, minerals and volatile oil analysis of Zanthoxylum acanthopodium DC. fruits

Combining ion chromatography with mass spectrometry and inductively coupled plasma‐mass spectrometry: Annual review 2020

Contact Info

Product

Resources

About